Articles
  • Comparison of the microstructure and compressive strength of Type 1 Portland cement paste between accelerated curing methods by microwave energy and autoclaving, and a saturated-lime deionized water curing method
  • Natt Makula,* and Dinesh Agrawalb
  • a Department of Construction Technology, Faculty of Industrial Technology, Phranakhon Rajabhat University, Changwattana Road, Bangkhen Bangkok 10220, Thailand b Materials Research Institute, The Pennsylvania State University, University Park, PA 16802, USA
Abstract
The microstructure and compressive strength of a 0.38 water-to-cement mass ratio (w/c) cement paste when subjected to accelerated-curing by microwave energy and autoclave curing were compared with a normal curing method by soaking in saturated-lime deionized water at 25 oC. The morphology, atom ratio of Si/Ca versus Al/Ca, phase composition by XRD, and compressive strength were measured in this study. The results indicate the presence of needle-like ettringite (Aft) in pastes that had been cured using the autoclave method. However, the saturated-lime deionized water cured paste showed lath-like or plate-like shapes and did not appear to produce ettringite (Aft). In addition, the microwave-cured paste indicated some evidence of ettringite. The range of Si/Ca and Al/Ca ratios of the autoclave-cured paste were 0.039− 0.052, and 0.207 − 0.234, respectively, while in the microwave-cured paste the ratio shifted to 0.079− 0.091. The compressive strength of the autoclavecured cement paste showed an increase in strength at an early age, while the strength decreased after 7 days of hydration.

Keywords: Autoclave curing, Cement paste, Compressive strength, Microwave accelerated curing, Microstructure.

This Article

  • 2012; 13(2): 174-177

    Published on Apr 30, 2012

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