Articles
  • Effect of Na2CO3 contents on synthesis of plate-like NaNbO3 particles for templated grain growth
  • Min-Soo Kima,*, Sung-Chan Leea, Sin-Woong Kima, Soon-Jong Jeonga, In-Sung Kima, Jae-Sung Songa, Jin-Joong Sohb and Woo-Bong Byunb
  • a Battery Research Center, Korea Electrotechnology Research Institute, Changwon, Korea b Electric Apparatus Testing Department, Korea Electrotechnology Research Institute, Changwon, Korea
Abstract
x mol% (x = 0 similar to 20) Na2CO3 excess Bi2.5Na3.5Nb5O18 (BNN) particles were synthesized using molten salt as a flux. The secondary phases were observed at stoichiometric ratio of BNN precursors and their intensity decreased with increasing Na contents. The results of SEM images showed that all particles existed in a platelet shape and the particle increased in size with higher increasing Na contents. Plate-like NaNbO3 particles were developed using BNN precursor obtained by a topochemical microcrystal conversion. XRD analysis of NaNbO3 particles showed that a single perovskite phase and the intensity of (h00) peaks increased with increasing Na contents in BNN precursor. SEM images showed that the size of plate-like NaNbO3 was significantly changed by controlling Na contents in BNN precursors.

Keywords: Template; NKN; NaNbO3; BNN; TMC method

This Article

  • 2012; 13(S2): 270-273

    Published on Nov 30, 2012

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